Chemistry · Solutions

Ideal & Non-Ideal Solutions, Azeotropes

Once Raoult's law gives us the vapour pressure a binary liquid mixture ought to have, the next question is whether real mixtures actually obey it. NCERT §1.5 sorts liquid–liquid solutions into ideal solutions, which follow Raoult's law at every composition, and non-ideal solutions, which deviate above or below it. This sub-topic — and the azeotropes it leads to — is among the most consistently examined in the Solutions chapter, with NEET 2020 and NEET 2025 both setting deviation questions outright.

Ideal Solutions

A liquid–liquid solution is classified using the yardstick of Raoult's law. The solutions which obey Raoult's law over the entire range of concentration are known as ideal solutions. For every composition, the partial vapour pressure of each component equals its mole fraction in the liquid times the vapour pressure of that pure component, and the total vapour pressure varies linearly between the two pure-liquid values.

For a two-component system of A and B, the defining relations are written compactly as follows, where $p_A^{\circ}$ and $p_B^{\circ}$ are the vapour pressures of the pure liquids:

$$p_A = x_A\,p_A^{\circ}, \qquad p_B = x_B\,p_B^{\circ}, \qquad p_{\text{total}} = x_A\,p_A^{\circ} + x_B\,p_B^{\circ}$$

Beyond obeying this law, ideal solutions carry two further signature properties. The enthalpy of mixing of the pure components to form the solution is zero, and the volume of mixing is also zero:

$$\Delta_{\text{mix}}H = 0, \qquad \Delta_{\text{mix}}V = 0$$
mole fraction → (x_A = 1 at left, x_B = 1 at right) vapour pressure p°_A p°_B p_total (linear) p_A = x_A p°_A p_B = x_B p°_B
Figure 1. An ideal solution. Each partial pressure (teal, purple) is a straight Raoult line, and the total vapour pressure (coral) is their straight-line sum lying between $p_A^{\circ}$ and $p_B^{\circ}$. There is no bulge above or sag below the line at any composition.

A perfectly ideal solution is rare, but several mixtures are nearly ideal because the two molecules are so alike. NCERT lists the solution of $\ce{n-hexane}$ and $\ce{n-heptane}$, the mixture of bromoethane $\ce{C2H5Br}$ and chloroethane $\ce{C2H5Cl}$, and the classic pairing of benzene $\ce{C6H6}$ and toluene $\ce{C6H5CH3}$ as members of this category.

Why Mixing Is Thermoneutral

The thermodynamic signatures of an ideal solution follow directly from molecular interactions. In the pure components only A–A and B–B attractions exist. On mixing, a new A–B interaction appears alongside them. Ideal behaviour is the special case where these three are essentially identical in strength.

When the intermolecular attractive forces between A–A and B–B are nearly equal to those between A–B, no extra energy is needed to pull like molecules apart and none is released when unlike molecules come together. Consequently no heat is absorbed or evolved on mixing ($\Delta_{\text{mix}}H = 0$), and because the packing is unchanged the volume of the solution is simply the sum of the volumes of the two components ($\Delta_{\text{mix}}V = 0$). The escaping tendency of each molecule in the mixture is exactly what it was in the pure liquid scaled by its mole fraction — which is precisely Raoult's law.

Build the foundation first

Deviations only make sense once the baseline law is solid. Revisit Raoult's Law for the partial-pressure relation that ideal solutions obey at every composition.

Non-Ideal Solutions and Deviation

When a solution does not obey Raoult's law over the entire range of concentration, it is called a non-ideal solution. The vapour pressure of such a solution is either higher or lower than the value predicted by Raoult's law. If it is higher, the solution exhibits positive deviation; if it is lower, it exhibits negative deviation. Most real solutions are, in fact, non-ideal to some degree.

The cause of these deviations lies entirely in the relative strengths of the molecular interactions. The whole topic reduces to comparing the A–B force against the A–A and B–B forces — a comparison that simultaneously fixes the sign of the deviation, the sign of $\Delta_{\text{mix}}H$, and the sign of $\Delta_{\text{mix}}V$.

composition (a) positive deviation observed > ideal composition (b) negative deviation observed < ideal
Figure 2. The two non-ideal cases against the dashed ideal (Raoult) line. (a) In positive deviation the observed total vapour pressure bulges above the Raoult line. (b) In negative deviation it sags below. The maximum or minimum of the observed curve fixes the azeotrope composition.

Positive Deviation

In a solution showing positive deviation from Raoult's law, the A–B interactions are weaker than those between A–A or B–B. The intermolecular attractive forces between the solute–solvent molecules are weaker than those among the solute–solute and solvent–solvent molecules. Molecules of A (or B) therefore find it easier to escape than in the pure state, so the vapour pressure rises and the observed value lies above the Raoult prediction. Because energy must be supplied to weaken the average attraction, $\Delta_{\text{mix}}H > 0$ (endothermic), and the loosened packing gives $\Delta_{\text{mix}}V > 0$.

The textbook example is a mixture of ethanol and acetone. In pure ethanol the molecules are hydrogen bonded. On adding acetone, its molecules get in between the host molecules and break some of those hydrogen bonds, weakening the overall interaction:

$$\ce{C2H5OH \cdots HOC2H5} \;\xrightarrow{\text{add }\ce{CH3COCH3}}\; \text{H-bonds broken} \;\Rightarrow\; \text{vapour pressure rises}$$

A second example NCERT gives is carbon disulphide added to acetone, $\ce{CS2}$ + $\ce{CH3COCH3}$, where the dipolar interactions between solute and solvent are weaker than the interactions among like molecules; this mixture also shows positive deviation. The familiar ethanol + water system behaves the same way.

Worked check

A solution of liquids X and Y has an observed total vapour pressure of 70 torr, while the Raoult's-law prediction works out to 73 torr. What deviation does it show?

Observed (70) is less than the calculated ideal value (73), so the vapour pressure has been suppressed: the mixture shows negative deviation. Had the observed value exceeded the predicted one, it would have been positive deviation. This is exactly the reasoning NEET set in 2025 (see PYQ snapshot below).

Negative Deviation

In a solution showing negative deviation, the intermolecular attractive forces between A–A and B–B are weaker than those between A–B. The new A–B interaction is the strongest of the three, so it decreases the escaping tendency of both components, lowers the vapour pressure, and pulls the observed value below the Raoult line. Here heat is released on mixing, $\Delta_{\text{mix}}H < 0$ (exothermic), and the tighter packing gives $\Delta_{\text{mix}}V < 0$.

The standard example is a mixture of chloroform and acetone. The chloroform molecule forms a hydrogen bond with the acetone molecule, an attraction absent in either pure liquid:

$$\ce{Cl3C-H \cdots O=C(CH3)2}$$

A second NCERT example is the mixture of phenol $\ce{C6H5OH}$ and aniline $\ce{C6H5NH2}$, where the hydrogen bond between the phenolic proton and the lone pair on the nitrogen of aniline is stronger than the hydrogen bonding between like molecules. The widely used nitric-acid–water mixture is another negative-deviation system.

Master Comparison Table

The three cases line up cleanly when read against one another. Memorise this grid as a single block — the sign of the deviation, the sign of $\Delta_{\text{mix}}H$ and $\Delta_{\text{mix}}V$, and the azeotrope type all move together.

Property Ideal solution Positive deviation Negative deviation
Raoult's law Obeyed at all compositions Not obeyed; $p_{\text{obs}} > p_{\text{Raoult}}$ Not obeyed; $p_{\text{obs}} < p_{\text{Raoult}}$
A–B vs A–A, B–B forces $A\text{–}B \approx A\text{–}A \approx B\text{–}B$ $A\text{–}B$ weaker than $A\text{–}A$, $B\text{–}B$ $A\text{–}B$ stronger than $A\text{–}A$, $B\text{–}B$
$\Delta_{\text{mix}}H$ = 0 > 0 (endothermic) < 0 (exothermic)
$\Delta_{\text{mix}}V$ = 0 > 0 < 0
Escaping tendency Unchanged Increased (escapes more easily) Decreased (escapes less easily)
NCERT examples $\ce{C6H6}$ + $\ce{C6H5CH3}$; $\ce{n-hexane}$ + $\ce{n-heptane}$ $\ce{C2H5OH}$ + $\ce{CH3COCH3}$; $\ce{CS2}$ + $\ce{CH3COCH3}$; ethanol + water $\ce{CHCl3}$ + $\ce{CH3COCH3}$; phenol + aniline; $\ce{HNO3}$ + water
Azeotrope formed None Minimum-boiling azeotrope Maximum-boiling azeotrope

Azeotropes

Some liquids on mixing form azeotropes, which are binary mixtures having the same composition in the liquid and the vapour phase and which boil at a constant temperature. Because the vapour leaving the boiling liquid has exactly the same composition as the liquid, distilling it does not change the proportions — so it is not possible to separate the components of an azeotrope by fractional distillation. There are two kinds.

Solutions that show a large positive deviation from Raoult's law form a minimum-boiling azeotrope at a specific composition. The ethanol–water mixture obtained by fermentation of sugars is the classic case: on fractional distillation it yields a solution of roughly 95% ethanol by volume, and once this azeotropic composition is reached the liquid and vapour have the same composition so no further separation occurs.

Solutions that show a large negative deviation form a maximum-boiling azeotrope at a specific composition. Nitric acid and water is the standard example, with an azeotrope of approximately 68% nitric acid and 32% water by mass that boils at 393.5 K.

composition boiling pt minimum-boiling positive devn. composition maximum-boiling negative devn.
Figure 3. Boiling-point–composition curves. A large positive deviation (low vapour pressure suppression failure) gives a boiling-point minimum — a minimum-boiling azeotrope (e.g. ethanol–water). A large negative deviation gives a boiling-point maximum — a maximum-boiling azeotrope (e.g. nitric acid–water). The azeotrope sits at the turning point.
NEET Trap

Match the deviation to the right azeotrope

The most frequent slip is pairing the deviations with the wrong azeotrope. High vapour pressure means the mixture boils more easily (lower boiling point), so positive deviation gives a minimum-boiling azeotrope. Low vapour pressure means it boils with difficulty (higher boiling point), so negative deviation gives a maximum-boiling azeotrope.

Positive deviation ($\Delta_{\text{mix}}H > 0$) → minimum-boiling azeotrope (e.g. ethanol–water, ~95% ethanol). Negative deviation ($\Delta_{\text{mix}}H < 0$) → maximum-boiling azeotrope (e.g. $\ce{HNO3}$–water, ~68% acid, 393.5 K).

Quick Recap

Six lines before the exam

  • Ideal solution: obeys Raoult's law at all compositions, with $\Delta_{\text{mix}}H = 0$ and $\Delta_{\text{mix}}V = 0$; A–B forces ≈ A–A ≈ B–B.
  • Near-ideal examples: $\ce{C6H6}$ + $\ce{C6H5CH3}$, $\ce{n-hexane}$ + $\ce{n-heptane}$, bromoethane + chloroethane.
  • Positive deviation: A–B weaker → $p_{\text{obs}} > p_{\text{Raoult}}$, $\Delta_{\text{mix}}H > 0$, $\Delta_{\text{mix}}V > 0$; e.g. ethanol + acetone, ethanol + water.
  • Negative deviation: A–B stronger → $p_{\text{obs}} < p_{\text{Raoult}}$, $\Delta_{\text{mix}}H < 0$, $\Delta_{\text{mix}}V < 0$; e.g. acetone + chloroform, phenol + aniline.
  • Azeotrope: same composition in liquid and vapour, boils at constant T, cannot be separated by fractional distillation.
  • Positive → minimum-boiling azeotrope; negative → maximum-boiling azeotrope.

NEET PYQ Snapshot — Ideal & Non-Ideal Solutions, Azeotropes

Real NEET questions on deviation from Raoult's law and ideal vapour pressure. Recurs almost every alternate year.

NEET 2025 · Q.90

5 moles of liquid X and 10 moles of liquid Y make a solution having a vapour pressure of 70 torr. The vapour pressures of pure X and Y are 63 torr and 78 torr respectively. Which of the following is true regarding the described solution?

  1. The solution has volume greater than the sum of individual volumes.
  2. The solution shows positive deviation.
  3. The solution shows negative deviation.
  4. The solution is ideal.
Answer: (3) Negative deviation

$x_X = \tfrac{5}{15}$, $x_Y = \tfrac{10}{15}$. Raoult prediction: $p_{\text{total}} = \tfrac{5}{15}(63) + \tfrac{10}{15}(78) = 21 + 52 = 73$ torr. The observed 70 torr is less than 73 torr, so the vapour pressure is suppressed — negative deviation.

NEET 2020 · Q.166

The mixture which shows positive deviation from Raoult's law is:

  1. Benzene + Toluene
  2. Acetone + Chloroform
  3. Chloroethane + Bromoethane
  4. Ethanol + Acetone
Answer: (4) Ethanol + Acetone

Adding acetone to ethanol breaks ethanol's hydrogen bonds, weakening the average interaction so molecules escape more easily and vapour pressure rises — positive deviation. Benzene + toluene and chloroethane + bromoethane are near-ideal; acetone + chloroform is negative deviation.

NEET 2021 · Q.95

The vapour pressure of a solution at 45°C with benzene to octane in molar ratio 3 : 2 is: [At 45°C $p^{\circ}$(benzene) = 280 mm Hg, $p^{\circ}$(octane) = 420 mm Hg; assume ideal behaviour]

  1. 350 mm Hg
  2. 160 mm Hg
  3. 168 mm Hg
  4. 336 mm Hg
Answer: (4) 336 mm Hg

For an ideal solution Raoult's law applies directly: $p_s = 280\times\tfrac{3}{5} + 420\times\tfrac{2}{5} = 168 + 168 = 336$ mm Hg. This is the baseline an ideal solution must obey before any deviation question makes sense.

NEET 2016 · Q.30

Which statement about the composition of the vapour over an ideal 1 : 1 molar mixture of benzene and toluene is correct at 25°C? [$p^{\circ}$(benzene) = 12.8 kPa, $p^{\circ}$(toluene) = 3.85 kPa]

  1. The vapour will contain a higher percentage of toluene
  2. The vapour will contain equal amounts of benzene and toluene
  3. Not enough information is given to make a prediction
  4. The vapour will contain a higher percentage of benzene
Answer: (4) Higher percentage of benzene

Benzene + toluene is an ideal solution. Since the liquid mole fractions are equal, the mole fraction of each component in the vapour is proportional to its pure-liquid vapour pressure. Benzene's $p^{\circ}$ (12.8 kPa) far exceeds toluene's (3.85 kPa), so the vapour is richer in the more volatile benzene.

FAQs — Ideal & Non-Ideal Solutions, Azeotropes

Common doubts on deviation, mixing thermodynamics, and azeotropes, answered from NCERT §1.5.

What is the difference between an ideal and a non-ideal solution?

An ideal solution obeys Raoult's law over the entire range of concentration and is formed with zero enthalpy of mixing and zero volume of mixing, because the A-B interactions are nearly equal to the A-A and B-B interactions. A non-ideal solution does not obey Raoult's law over the whole concentration range; its observed vapour pressure is either higher (positive deviation) or lower (negative deviation) than the Raoult's law prediction, and its enthalpy and volume of mixing are non-zero.

Why does an ethanol and water mixture show positive deviation from Raoult's law?

In pure ethanol the molecules are held by hydrogen bonds. When a second component is added, its molecules get in between the host molecules and break some of these hydrogen bonds, so the A-B interactions become weaker than the A-A and B-B interactions. The molecules therefore escape more easily than in the pure state, the observed vapour pressure rises above the Raoult's law value, and the solution shows positive deviation.

Why does an acetone and chloroform mixture show negative deviation?

Chloroform forms a new hydrogen bond with acetone, so the A-B attractive force is stronger than the A-A and B-B forces. This reduces the escaping tendency of both components, the observed vapour pressure falls below the Raoult's law value, and the solution shows negative deviation from Raoult's law.

What is an azeotrope and why can it not be separated by fractional distillation?

An azeotrope is a binary mixture that has the same composition in the liquid and the vapour phase and boils at a constant temperature. Because the vapour produced has exactly the same composition as the boiling liquid, distilling it does not enrich either component, so the two liquids cannot be separated from one another by fractional distillation.

How are positive and negative deviation linked to the two types of azeotrope?

Solutions that show a large positive deviation from Raoult's law form a minimum-boiling azeotrope at a specific composition, for example the ethanol-water mixture that distils as roughly 95% ethanol by volume. Solutions that show a large negative deviation form a maximum-boiling azeotrope, for example nitric acid and water, which forms an azeotrope of about 68% nitric acid and 32% water by mass boiling at 393.5 K.

Name some solutions that behave almost ideally.

A perfectly ideal solution is rare, but several mixtures are nearly ideal because the two kinds of molecule are very similar in size and intermolecular force. NCERT lists the solution of n-hexane and n-heptane, the mixture of bromoethane and chloroethane, and the benzene and toluene mixture as examples that fall into this category.